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Ch 313W - Instrumental Analysis, S '14

hp_gc-ms.gif (13001 bytes)
Agilent Technologies GC-MS

A study of the use of instrumental methods for qualitative and quantitative analyses of  unknown chemical samples. Important applications to the fields of Chemistry and Biology are emphasized. In addition, since this is a writing intensive course, formal lab write-ups are required in the style of a technical journal article.

PerkinElmer Spectrum Spotlight 200 FTIR Microscope System



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Instructor:
Dr. Pete Poston
office: NS 110
phone:503-838-8218
office hours: MWF 10, MF 2, make an appointment, or just drop by.
web page: http://www.wou.edu/poston
email questions: postonp@wou.edu
Pre-req's Ph 213/Ph 203 and MTH 251
Textbook Skoog, Holler, & Crouch, "Principles of Instrumental Analysis", 6th ed.
Calculators
A scientific calculator is mandatory. You must come prepared for every quiz, midterm, and final with your own calculator. I will not loan out calculators, and you are not allowed to borrow one from another student while testing.
Cell Phones and Computers

I have mixed feelings about smart devices - they can be a valuable educational resource, but texting, etc is discouraged. What's the point to coming to class if you aren't paying attention?

However, from time to time I will recommend interesting, educational, and fun app's and will use them in lectures and during the recitation. Feel free to download them at that time.

Cell phones need to be either turned off or placed in vibrate mode during lecture. If I see you using one of these devices during testing, I will consider it cheating and give you a zero.

Lab & Formal Write-ups I will furnish all lab handouts. In addition, purchase some kind of storage device (USB flash drive, etc) for data and reports. Every lab has a handout that must be turned in at the end of the lab (you will receive photocopies so that you can work on the associated writing assignment for that lab). There is no lab notebook.

You will learn how to write in the style of a technical journal article. Technical articles in chemistry commonly contain the following sections: (1) Abstract, (2) Introduction, (3) Experimental, (4) Results & Discussion, (5) Conclusion, and (6) References. You will receive handouts explaining the various sections. As shown in the table below, different labs have different sections as the formal writing component. In lab #9 - GC-MS - you will submit a complete formal writeup containing all sections.

There is also a 10 pt writing exercise that emphasizes style issues and illustrates some of the common writing mistakes that I have observed over the years.

All labs are due one week later at 5 PM (e.g. a Tuesday lab means due next Tuesday at 5 PM). The only exception is if there is a Ch 313 exam or university holiday on the due day, in which case the lab is due at 5 PM the next day the university is open.

All writing assignments must be written in Microsoft Word and submitted digitally via email. I then make editorial comments and email it back to you so you can see the changes.

When I give a grade on writing assignments, I give a subjective grade (A+ through F) where the point values are: A+ = 100%, A = 95%, B = 85%, C = 75%, D = 65%, F = write over

Here are the labs that have a formal writing component (see table below for dates):

Lab #2 - Monochromators - Abstract
Lab #3 - UV-Vis - Introduction
Lab #5 - Atomic Absorption Spectroscopy - Experimental Section
Lab #6 - Fourier Transform Infrared Spectroscopy - Results & Discussion, Conclusions
Lab #8 - Gas Chromatography-Mass Spectrometry - complete formal lab including references

The point breakdown for each lab is -

Tuesday
Lab
Handout
Formal Writing
Total
Apr 15 Lab #2 - Monochromators 5 pts Abstract - 5 pts 10 pts
Apr 22 Lab #3 - UV-Vis 5 pts Introduction - 10 pts 15 pts
Apr 29 Lab #4 - Fluorescence 5 pts

---

5 pts
May 6 Lab #5 - Atomic Absorption Spectroscopy 5 pts Experimental - 5 pts 10 pts
May 13 Lab #6 - Fourier Transform Infrared Spectroscopy 5 pts Results & Discussion, Conclusions - 10 pts 15 pts
May 20 Lab #7 - Raman Spectroscopy 5 pts

---

5 pts
May 27 Lab #8 - Gas Chromatography-Mass Spectrometry 5 pts complete formal lab writeup - 30 pts 35 pts
Jun 3 Lab #9 - High Performance Liquid Chromatography 5 pts   5 pts
TOTAL   100 pts
Late Labs

Labs must be turned in on time or else chaos ensues! The following "late fees" will be assessed starting at 8 AM the day following the due date:

1 day late = 1/4 off, 2 days late = 1/2 off, 3 days late = 3/4 off

You will receive a zero for all labs more than 3 days late. No labs will be accepted past the last day of classes.

SInce this is a writing-intensive course, failure to hand in any lab handout or writing assignment will result in failing the course.

Quizzes

There will be eight 10 min quizzes given at the beginning of each lab related to the lab topic that week.

Each quiz is worth 10 pts, and the questions are usually a reworked homework problem. Links to homework answer keys are available online as Adobe PDF files and can be found in the Syllabus section below.

Your lowest quiz score will be dropped. Since the lowest quiz score is being dropped anyway, there will be no make-ups on quizzes. If you miss three quizzes total (including the one you drop), then you fail the class.

Make-ups

There are no make-up exams except for University sanctioned events, in which case please see me a week in advance for an alternative testing time. In the event of an unexpected emergency, then -

Midterms: Family-related emergencies or deaths must be communicated through the Office of Student Affairs (838-8221) and broadcast to all your professors. Illnesses must be accompanied by a note from your doctor. Under these conditions there are two options for replacing the midterm score:

(1) If the exam hasn't been handed back to the class yet, then arrange a make-up time with me.

(2) If the exam has already been returned to the class, then I will replace the missing hour exam score by taking 30% of the percentage you receive on the final exam (since it is a 200 pt exam) and 40% of the other midterm score. This option can obviously only be used once.

Final exam: University policy states that the final exam time will not be moved for any reason. Please do not ask to take the final early because you want to leave for vacation early! There are humanitarian exceptions - see me if there's a problem. Again, if you miss the final and follow the same procedure listed above under midterms, then I will give you an incomplete and you can take the final in a future class section to make it up (see Incompletes section below).

Homework Assigned, key posted, but not graded. I guarantee one or two will appear on exams, however!
Grading
200 pts (33%) two 100 pt hour exams (Thur, Apr 24 and Thur, May 22)
200 pts (33%) 200 pt comprehensive final (Tue, Jun 12, 8-10 AM)
100 pts (17%) 8 quizzes @ 10 pts each - score scaled to 100 pts total
100 pts (17%) labs and written reports (100 pts), writing exercise (10 pts), total scaled to 100 pts.
600 pts total

Grading will be no harder than 90% A, 80% B, 70% C, 60% D, < 60% F

Incompletes Incompletes are given under special circumstances such as medical reasons, family emergencies, etc. In order to receive an incomplete, you must sign a contract with me outlining the steps you must take to finish the course. Usually this means there will be a time deadline for completion of the course.
Students with Disabilities It is your right to request special accommodations under the Americans with Disabilities Act. For questions, call the Office for Disability Services at (503) 838-8250 V/TTY, or email them at ods@wou.edu.


COURSE SYLLABUS

Click here for the reading and Homework Problems for the 5th ed. of the Text

Dates (Tue) Chapter Topic/Links Lab and Writing Assignments
Apr 1

Reading:
Ch 1: p.2-3, p. 17-22
Ch 6: p. 132-142, 152-159

Problem Set 1:
Ch 1: 12de
Ch 6:
1e-j, 5-7

Intro, Statistics & Detection Limits

Electromagnetic Radiation

Technical Writing Guidelines

Extra Lecture Time

Apr 8

Reading:
Ch 7: p. 164-166, 175-202

Problem Set 2:
Ch 7: 1, 12-14, 19

Instruments in Optical Spectroscopy

Extra lecture time

Lab #1:
Interfacing instruments using LabView

Apr 15

Reading:
Ch 13: p. 336-343, 346-362
Ch 14: p. 367-370

Problem Set 3:
Ch 13: 1d, 2a, 5, 8ab, 13abdfgh, 14ab, 15, 20abcf
Ch 14: 11ab, 12b

Introduction to Absorption Spectroscopy

Applications of UV-Vis Spectroscopy

LAB #2: Monochromators
(Abstract)

Apr 22*

Reading:
Ch 15: p. 399-418
Ch 1: p. 13-17

Problem Set 4:
Ch 15: 1-4, 8

EXAM #1 - Thur Apr 24

Fluorescence & Phosphorescence

LAB #3: UV-Vis
(Introduction)

Apr 29

Reading:
Ch 8: p. 215-223
Ch 9: p. 230-248
Ch 10: p. 254-269
Ch 12: p. 303-319

Problem Set 5:
Ch 8: 8
Ch 9: 1a-f,i-j,l, 3, 5, 8, 11, 13, 14
Ch 10: 2, 4
Ch 12: 1, 2d, 9c

Atomic Absorption Spectroscopy

ICP Spectroscopy

Atomic X-Ray Spectrometry

LAB #4: Fluorescence

May 6

Reading:
Ch 7: p. 204-211
Ch 16:
p. 430-444
Ch 17: p. 455-472
Ch 18: p. 481-492

Problem Set 6:
Ch 16: 1, 3, 6, 7,8,9a
Ch 18: 1-2, 6, 9a

Infrared Spectroscopy, FT-IR and applications

Raman Spectroscopy

LAB #5: Atomic Absorption Spectroscopy
(Experimental)

May 13

Reading:
Ch 19: p. 498-519, 521-532
Ch 20: p. 550-573

Problem Set 7: (©Thompson Brooks Cole)
Ch 19: 3, 5, 6, 7ab, 23, 25, 28, 33
Ch 20: 2, 10, 17, 18

NMR Spectroscopy

Mass Spectrometry

LAB #6: Fourier Transform Infrared Spectroscopy
(Results & Discussion, Conclusions)

May 20 ---

EXAM #2 - Thur May 22

Mass Spectrometry cont'd

LAB #7: Raman Spectroscopy

May 27

Reading:
Ch 26: p. 762-781
Ch 27: p. 788-807

Problem Set 8: (©Thompson Brooks Cole)
Ch 26: 1, 3, 6, 7, 11, 14, 15a, 16ab
Ch 27:
3, 11, 12, 16, 17, 20, 27cdef

No class Thur, May 29th for Academic Excellence Showcase

Intro to Chromatography

Gas Chromatography

LAB #8: Gas Chromatography-Mass Spectrometry
(complete formal lab writeup)

Jun 3

Reading:
Ch 28: p. 816-837
Ch 30: p. 867-877

Problem Set 9: (©Thompson Brooks Cole)
Ch 28: 4, 7abdej, 10, 11

GC-MS

HPLC

LAB #9: High Performance Liquid Chromatography

*Last day to drop without being responsible for a grade is Friday, Apr 25

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This page last modified on Wed Mar 26 2008 16:09:35 GMT-0700 (Pacific Daylight Time)